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制备SNS钴（II）针质模型复合物肝酒精脱氢酶
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Preparation of SNS Cobalt(II) Pincer Model Complexes of Liver Alcohol Dehydrogenase
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制备SNS钴（II）针质模型复合物肝酒精脱氢酶

DOI:
10.3791/60668-v

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06:31 min

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March 19, 2020

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, , , , , , ,
1Department of Chemistry and Biochemistry,Fairfield University, 2Department of Chemistry,Keene State College

Chapters

  • 00:04Introduction
  • 00:52Chloro-(n3-S,S,N)-[2,6-bis(N-isopropyl-N -methyleneimidazole-2-thione)pyridine]cobalt(II)tetrachlorocobaltate [4] Synthesis
  • 01:42Chloro-(n3-S,S,N)-[2,6-bis(N-isopropyl-N -methyleneimidazole-2-thione)pyridine]cobalt(II)tetrachlorocobaltate [4] Recrystallization
  • 02:34Chloro-(n3-S,S,N)-[2,6-bis(N-isopropyl-N -methylenetriazole-2-thione)pyridine]cobalt(II)tetrachlorocobaltate [5] Synthesis
  • 03:22Chloro-(n3-S,S,N)-[2,6-bis(N-isopropyl-N’-methylenetriazole-2-thione)pyridine]cobalt(II) tetrachlorocobaltate [5] Recrystallization
  • 04:28Results: Representative Liver Alcohol Dehydrogenase Complex Analyses
  • 05:41Conclusion

Summary

자동 번역

자동 번역

介绍了肝酒精脱氢酶SNS针质钴（II）模型复合物的制备情况。复合物可以通过用CoCl2+6H2O对配体前体进行反应来制备，然后通过允许二苯醚缓慢扩散到含有钴复合物的醋酸酯溶液中来重新结晶。

Tags

Cobalt(II) PincerLiver Alcohol DehydrogenaseSingle Crystal GrowthAcetonitrileRefluxRotary EvaporationVapor Diffusion26-BIS-N-isopropyl-N’-methyleneimidzole-2-thione-pyridine26-BIS-N-isopropyl-N’-methylenetriazole-2-thione-pyridineCobalt(II) Chloride HexahydrateTetrachlorocobaltate

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