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Nの準備-(2-alkoxyvinyl) N- トシル-1,2,3-トリアゾールと置換 Phthalans とフェネチルアミンに後続の変換からサルファ剤
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JoVE Journal Chemistry
Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines
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Nの準備-(2-alkoxyvinyl) N- トシル-1,2,3-トリアゾールと置換 Phthalans とフェネチルアミンに後続の変換からサルファ剤

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9,541 Views

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10:42 min

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January 03, 2018

DOI:

10.3791/56848-v

DOI:
10.3791/56848-v

•

10:42 min
January 03, 2018

•

3 Views
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1Chemistry Department,Hamilton College

Summary

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Nの合成についての代表的な実験-(2-alkoxyvinyl) サルファ剤と phthalan とフェネチルアミン誘導体とそれに続く変換詳細でご紹介します。

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Keyword Extraction:N-(2-alkoxyvinyl)sulfonamidesN-tosyl-123-triazolesPhthalansPhenethylamines2-ethynylbenzyl AlcoholCopper-thiophene-carboxylateP-Toluenesulfonyl AzideMicrowave ReactorSilica GelFlash ChromatographyTriazole Product

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Bennett, J. M., Shapiro, J. D., Choinski, K. N., Mei, Y., Aulita, S. M., Dominguez, G. M., Majireck, M. M. Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines. J. Vis. Exp. (131), e56848, doi:10.3791/56848 (2018).

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