Journal
/
화학
/
Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines
JoVE 신문
화학
JoVE 비디오를 활용하시려면 도서관을 통한 기관 구독이 필요합니다.  전체 비디오를 보시려면 로그인하거나 무료 트라이얼을 시작하세요.
JoVE 신문 화학
Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines

Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines

DOI:
10.3791/56848-v

•

10:42 min

•

January 03, 2018

•

, , , , , ,
1Chemistry Department,Hamilton College

Chapters

  • 00:05Title
  • 00:48Synthesis of N-Tosyl Triazole 2a:2-(1-tosyl-1H-1,2,3 triazol-4-yl)phenyl Methanol
  • 03:03Synthesis of N-(2-alkoxyvinyl)sulfonamide Phthalan 3a: (Z)-N-(isobenzofuran-1(3H)-ylidenemethyl)-4-methylbenzenesulfonamide
  • 04:14Synthesis of Phthalan 4: N-((1,3-dihydroisobenzofuran-1-yl)methyl)-4-methylbenzenesulfonamide
  • 05:34Synthesis of Phenylthylamine 5: N-(2-(hydroxymethyl)phenethyl)-4-methylbenzenesulfonamide
  • 07:29Synthesis of Ketal 6c: N-((1-(2-hydroxyethoxy)-1,3-dihydroisobenzofuran-1-yl)methyl)-4-methybenzenesulfonamide
  • 08:12Results: Characterization of N-(2-alkoxyvinyl)sulfonamides and Derivatives
  • 10:00Conclusion

Summary

자동 번역

자동 번역

Representative experimental procedures for the synthesis of N-(2-alkoxyvinyl)sulfonamides and subsequent conversion to phthalan and phenethylamine derivatives are presented in detail.

Tags

Keyword Extraction:N-(2-alkoxyvinyl)sulfonamidesN-tosyl-123-triazolesPhthalansPhenethylamines2-ethynylbenzyl AlcoholCopper-thiophene-carboxylateP-Toluenesulfonyl AzideMicrowave ReactorSilica GelFlash ChromatographyTriazole Product

Article

Embed

플레이리스트에 추가

Usage Statistics

Related Videos

Nucleoside Triphosphates – From Synthesis to Biochemical Characterization

Preparation and Characterization of SDF-1α-Chitosan-Dextran Sulfate Nanoparticles

Preparation of Mica and Silicon Substrates for DNA Origami Analysis and Experimentation

Preparation and Characterization of Individual and Multi-drug Loaded Physically Entrapped Polymeric Micelles

Facile Preparation of 4-Substituted Quinazoline Derivatives

Laboratory Production of Biofuels and Biochemicals from a Rapeseed Oil through Catalytic Cracking Conversion

One-pot Microwave-assisted Conversion of Anomeric Nitrate-esters to Trichloroacetimidates

Preparation and Characterization of C60/Graphene Hybrid Nanostructures

The Effect of Ultraviolet Radiation on the Chemical Bath Deposition of Bis(thiourea) Cadmium Chloride Crystals and the Subsequent CdS Obtention

Tuning Oxide Properties by Oxygen Vacancy Control During Growth and Annealing

Read Article