Preparation of <em>N</em>-(2-alkoxyvinyl)sulfonamides from <em>N</em>-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines

John M. Bennett; Jonathan D. Shapiro; Krystina N. Choinski; Yingbin Mei; Sky M. Aulita; Giovanny M. Dominguez; Max M. Majireck

doi:10.3791/56848

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Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines

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化学

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JoVE Journal 化学

Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines

9,541 Views

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10:42 min

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January 03, 2018

DOI:

10.3791/56848-v

DOI:

10.3791/56848-v

•

10:42 min

January 03, 2018

•

3 Views

John M. Bennett¹, Jonathan D. Shapiro¹, Krystina N. Choinski¹, Yingbin Mei¹, Sky M. Aulita¹, Giovanny M. Dominguez¹, Max M. Majireck¹

¹Chemistry Department,Hamilton College

概要

Representative experimental procedures for the synthesis of N-(2-alkoxyvinyl)sulfonamides and subsequent conversion to phthalan and phenethylamine derivatives are presented in detail.

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Keyword Extraction:N-(2-alkoxyvinyl)sulfonamides N-tosyl-1 2 3-triazoles Phthalans Phenethylamines 2-ethynylbenzyl Alcohol Copper-thiophene-carboxylate P-Toluenesulfonyl Azide Microwave Reactor Silica Gel Flash Chromatography Triazole Product

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Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines

概要

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