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High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
Chapters
- 00:04Introduction
- 00:55Solid Sample Pretreatment
- 01:57Solid Sample Loading
- 02:52NMR Rotor Charging
- 04:58Magic Angle Spinning (MAS) NMR Experiment
- 05:46Results: Representative In Situ 1H and 13C MAS NMR Analyses
- 07:49Conclusion
The molecular structures and dynamics of solids, liquids, gases, and mixtures are of critical interest to diverse scientific fields. High-temperature, high-pressure in situ MAS NMR enables detection of the chemical environment of constituents in mixed phase systems under tightly controlled chemical environments.
