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Synthesis of Terpolymers at Mild Temperatures Using Dynamic Sulfur Bonds in Poly(S-Divinylbenzene)
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Synthesis of Terpolymers at Mild Temperatures Using Dynamic Sulfur Bonds in Poly(S-Divinylbenzene)

Synthesis of Terpolymers at Mild Temperatures Using Dynamic Sulfur Bonds in Poly(S-Divinylbenzene)

DOI:
10.3791/59620-v

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09:16 min

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May 20, 2019

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, ,
1Department of Chemistry,Ball State University

Chapters

  • 00:04Title
  • 01:06Synthesis of Poly(S-divinylbenzene)
  • 01:53Preparation of Terpolymers
  • 04:11Control Polymerizations, Polymer Characterization, and Solubility Studies
  • 06:41Results: Polysulfide Initiated Polymerization and Characterization of Terpolymers
  • 08:32Conclusion

Summary

자동 번역

자동 번역

The goal of this protocol is to initiate polymerization using dynamic sulfur bonds in poly(S-divinylbenzene) at mild temperatures (90 °C) without using solvents. Terpolymers are characterized by GPC, DSC and 1H NMR, and tested for changes in solubility.

Tags

PolysulfideInverse VulcanizationTerpolymerDynamic Sulfur BondsPoly(S-divinylbenzene)14-Cyclohexanedimethanol Divinyl EtherMaleimideMild Temperature Polymerization

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