Here, we present a protocol for performing in situ TEM closed-cell gas reaction experiments while detailing several commonly used sample preparation methods.
Unocic, K. A., Hensley, D. K., Walden, F. S., Bigelow, W. C., Griffin, M. B., Habas, S. E., Unocic, R. R., Allard, L. F. Performing In Situ Closed-Cell Gas Reactions in the Transmission Electron Microscope. J. Vis. Exp. (173), e62174, doi:10.3791/62174 (2021).