We present detailed procedures to produce experimental equilibrium curves of the phase composition as a function of solvent concentration in a solid state system under milling conditions.
Belenguer, A. M., Lampronti, G. I., Sanders, J. K. M. Reliable Mechanochemistry: Protocols for Reproducible Outcomes of Neat and Liquid Assisted Ball-mill Grinding Experiments. J. Vis. Exp. (131), e56824, doi:10.3791/56824 (2018).