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Reliable Mechanochemistry: Protocols for Reproducible Outcomes of Neat and Liquid Assisted Ball-mill Grinding Experiments
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Reliable Mechanochemistry: Protocols for Reproducible Outcomes of Neat and Liquid Assisted Ball-mill Grinding Experiments

Reliable Mechanochemistry: Protocols for Reproducible Outcomes of Neat and Liquid Assisted Ball-mill Grinding Experiments

DOI:
10.3791/56824-v

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13:05 min

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January 23, 2018

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, ,
1Department of Chemistry,University of Cambridge, 2Department of Earth Sciences,University of Cambridge

Capitoli

  • 00:05Titolo
  • 00:56Calibration of Electronic Air-Displacement Pipette in Reverse Pipetting Mode
  • 03:04Ball Mill Liquid-Assisted Grinding (LAG) Synthesis of 4-Chlorophenyl-2-nitrophenyl Disulfide (1-2) Using High-Affinity Solvent (17.0 μL Acetone)
  • 06:54Ball Mill LAG Synthesis of 1-2 Using a Low-Affinity Solvent (65 μL Methanol)
  • 09:46Results: Solvent Milling Equilibrium Curves for the Ball Mill LAG Synthesis of Heterodimer 1-2
  • 11:29Conclusion

Summary

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We present detailed procedures to produce experimental equilibrium curves of the phase composition as a function of solvent concentration in a solid state system under milling conditions.

Tags

MechanochemistryBall-mill GrindingLiquid-assisted Grinding (LAG)PolymorphismSolvent EffectsExperimental DesignReproducibilityPipette CalibrationEquilibrium Crystal Phase Composition

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