Journal
/
화학
/
Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy
JoVE 신문
화학
This content is Free Access.
JoVE 신문 화학
Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy

Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy

DOI:
10.3791/64316-v

•

07:20 min

•

January 20, 2023

•

, , , , , , , , , ,
1Institute of Energy and Climate Research – Fundamental Electrochemistry (IEK-9),Forschungszentrum Jülich GmbH, 2Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons,Forschungszentrum Jülich GmbH, 3Dyson School of Design Engineering,Imperial College London, 4Central Facility for Electron Microscopy (GFE),RWTH Aachen University, 5Institute of Physical Chemistry,RWTH Aachen University

Chapters

  • 00:04Introduction
  • 01:00Preparation of Half‐Cut TEM Grids with Coated Si Nanoparticles for Checking the Suitability of ALD‐Deposited Titanium Dioxide Coatings
  • 01:53Preparing the Tungsten Needle
  • 02:37Loading the Drop‐Casted TEM Grid and Lithium Loaded Tungsten Needle into the In Situ TEM Holder
  • 03:15Inserting the Assembled In Situ Holder into the TEM
  • 04:02Performing the In Situ Biasing Experiment in the TEM and Analyzing the TEM Images
  • 05:37Results: Screening Method of Potential Coatings for All‐Solid‐State Batteries Using In Situ Transmission Electron Microscopy
  • 06:28Conclusion

Summary

자동 번역

자동 번역

Utilizing the volume change of Si nanoparticles during (de)lithiation, the present protocol describes a screening method of potential coatings for all-solid-state batteries using in situ transmission electron microscopy.

Tags

Keywords: All-solid-state BatteryCoatingIn Situ TEMSilicon NanoparticlesLithiationDelithiationTitanium DioxideTungsten NeedleElectropolishingConductive Glue

Article

Embed

플레이리스트에 추가

Usage Statistics

Related Videos

check_url/kr/64316?article_type=v

Preparation of Highly Porous Coordination Polymer Coatings on Macroporous Polymer Monoliths for Enhanced Enrichment of Phosphopeptides
check_url/kr/64316?article_type=v

In Situ Monitoring of Diffusion of Guest Molecules in Porous Media Using Electron Paramagnetic Resonance Imaging
check_url/kr/64316?article_type=v

In Situ Characterization of Boehmite Particles in Water Using Liquid SEM
check_url/kr/64316?article_type=v

Liquid-cell Transmission Electron Microscopy for Tracking Self-assembly of Nanoparticles
check_url/kr/64316?article_type=v

Obtaining 3D Chemical Maps by Energy Filtered Transmission Electron Microscopy Tomography
check_url/kr/64316?article_type=v

An Experimental Protocol for Femtosecond NIR/UV – XUV Pump-Probe Experiments with Free-Electron Lasers
check_url/kr/64316?article_type=v

Microfluidic Chips for In Situ Crystal X-ray Diffraction and In Situ Dynamic Light Scattering for Serial Crystallography
check_url/kr/64316?article_type=v

Analysis of Minerals Produced by hFOB 1.19 and Saos-2 Cells Using Transmission Electron Microscopy with Energy Dispersive X-ray Microanalysis
check_url/kr/64316?article_type=v

Using Graphene Liquid Cell Transmission Electron Microscopy to Study in Situ Nanocrystal Etching
check_url/kr/64316?article_type=v

Performing Spectroscopy on Plasmonic Nanoparticles with Transmission-Based Nomarski-Type Differential Interference Contrast Microscopy

Read Article