的合成[锡 10（SI（SIME 3） 3） 4] 2</sup -使用亚稳锡（I）卤溶液通过共缩聚合成技术

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The Synthesis of [Sn₁₀(Si(SiMe₃)₃)₄]²^– Using a Metastable Sn(I) Halide Solution Synthesized via a Co-condensation Technique

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的合成[锡 10（SI（SIME 3） 3） 4] 2</sup -使用亚稳锡（I）卤溶液通过共缩聚合成技术

DOI:

10.3791/54498-v

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12:43 min

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November 28, 2016

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Mareike Binder, Claudio Schrenk, Andreas Schnepf

¹Chemistry Department, Institute of Inorganic Chemistry,University of Tübingen

Chapters

00:05Title
01:14Setup of the Graphite Reactor and Co-condensation Apparatus
04:48Co-condensation Reaction
08:59Synthesis of Sn₁₀(Hyp)₄^2-
09:57Results: Metastable Sn(I) Chloride Solution Obtained by Co-condensation Applied for Preparation of [Sn₁₀(Si(SiMe₃)₃)₄]^2-
10:51Conclusion

Summary

자동 번역

The disproportionation reaction of a metastable Sn(I) chloride solution, obtained via the preparative co-condensation technique, is used for the synthesis of a metalloid tin cluster compound.

的合成[锡<sub> 10</sub>（SI（SIME<sub> 3</sub>）<sub> 3</sub>）<sub> 4</sub>]<sup> 2</sup<sup> -</sup>使用亚稳锡（I）卤溶液通过共缩聚合成技术

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