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Performing In Situ Closed-Cell Gas Reactions in the Transmission Electron Microscope
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14:21 min
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July 24, 2021
DOI:
1Center for Nanophase Materials Sciences,Oak Ridge National Laboratory, 2Protochips Inc., 3Department of Materials Science & Engineering,University of Michigan, 4Catalytic Carbon Transformation & Scale-up,National Renewable Energy Laboratory, 5Materials Science & Technology Division,Oak Ridge National Laboratory
Summary
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Here, we present a protocol for performing in situ TEM closed-cell gas reaction experiments while detailing several commonly used sample preparation methods.
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Unocic, K. A., Hensley, D. K., Walden, F. S., Bigelow, W. C., Griffin, M. B., Habas, S. E., Unocic, R. R., Allard, L. F. Performing In Situ Closed-Cell Gas Reactions in the Transmission Electron Microscope. J. Vis. Exp. (173), e62174, doi:10.3791/62174 (2021).
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