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Methods of Ex Situ and In Situ Investigations of Structural Transformations
 

Methods of Ex Situ and In Situ Investigations of Structural Transformations: The Case of Crystallization of Metallic Glasses

Article DOI: 10.3791/57657-v • 08:55 min • June 7th, 2018
June 7th, 2018 •
1,2, 3, 3, 4, 4, 5
1Institute of Nuclear and Physical Engineering, Slovak University of Technology in Bratislava, Slovakia, 2Department of Nuclear Reactors, Czech Technical University in Prague, Czech Republic, 3Department of Experimental Physics, Palacky University Olomouc, Czech Republic, 4Institute of Physics, Slovak Academy of Sciences, Bratislava, Slovakia, 5Institute of Laboratory Research on Geomaterials, Faculty of Natural Sciences, Comenius University in Bratislava, Slovakia

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Here, we present a protocol to describe ex situ and in situ investigations of structural transformations in metallic glasses. We employed nuclear-based analytical methods which inspect hyperfine interactions. We demonstrate the applicability of Mössbauer spectrometry and nuclear forward scattering of synchrotron radiation during temperature-driven experiments.

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Ex Situ Investigations In Situ Investigations Structural Transformations Crystallization Metallic Glasses Nuclear-based Analytical Methods Hyperfine Interactions Mossbauer Spectroscopy Nuclear Forward Scattering Synchrotron Radiation Transient States Planar Flow Casting Amorphous Nature X-ray Diffraction Bragg-Brentano Geometry
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