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Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques
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JoVE Journal Ingenieurwesen
Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques

Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques

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10:03 min

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November 11, 2013

DOI:

10.3791/50594-v

DOI:
10.3791/50594-v

•

10:03 min
November 11, 2013

•

21 Views
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1Environmental Energy Technologies Division,Lawrence Berkeley National Laboratory, 2Department of Chemistry,University of Illinois at Chicago, 3Stanford Synchrotron Radiation Lightsource, 4Haldor Topsøe A/S, 5PolyPlus Battery Company

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We describe the use of synchrotron X-ray absorption spectroscopy (XAS) and X-ray diffraction (XRD) techniques to probe details of intercalation/deintercalation processes in electrode materials for Li-ion and Na-ion batteries. Both in situ and ex situ experiments are used to understand structural behavior relevant to the operation of devices

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Lithium Ion BatteriesSodium Ion BatteriesElectrode MaterialsSynchrotron RadiationX-ray DiffractionX-ray Absorption SpectroscopyIn Situ ExperimentsEx Situ ExperimentsIntercalation CompoundsTransition Metal OxidesPhosphatesRedox StatesPhase TransitionsLattice Parameters

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Doeff, M. M., Chen, G., Cabana, J., Richardson, T. J., Mehta, A., Shirpour, M., Duncan, H., Kim, C., Kam, K. C., Conry, T. Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques. J. Vis. Exp. (81), e50594, doi:10.3791/50594 (2013).

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