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February 20, 2020
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Here, we present a method for the observation of solution interactions between Lewis acids and bases by employing in situ infrared spectroscopy as a detector for titration under synthetically relevant conditions. By examining solution interactions, this method represents a complement to X-ray crystallography, and provides an alternative to NMR spectroscopy.
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Hanson, C. S., Devery, J. J. Characterizing Lewis Pairs Using Titration Coupled with In Situ Infrared Spectroscopy. J. Vis. Exp. (156), e60745, doi:10.3791/60745 (2020).
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