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利用光致硫醇-烯/yne Hydrothiolation 构造硫醚类/乙烯基硫化物栓系螺旋肽
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Constructing Thioether/Vinyl Sulfide-tethered Helical Peptides Via Photo-induced Thiol-ene/yne Hydrothiolation
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利用光致硫醇-烯/yne Hydrothiolation 构造硫醚类/乙烯基硫化物栓系螺旋肽

DOI:
10.3791/57356-v

•

11:09 min

•

August 01, 2018

•

, , ,
1Key Laboratory of Chemical Genomics, School of Chemical Biology and Biotechnology,Peking University Shenzhen Graduate School

Bölümler

  • 00:04Başlık
  • 00:38Manual Solid-Phase Peptide Synthesis
  • 02:42Formation of Thioether Linker by On-Resin Cyclization
  • 05:29Thioether Linker Formation via Intermolecular Thio-ene Reaction and Peptide Cyclization via Macrolactamization
  • 07:02Solution-Phase Formation of a Vinyl Sulfide Linker
  • 08:41Results: Thioether- and Vinyl Sulfide-Tethered Cyclic Peptides
  • 10:42Conclusion

Özet

Otomatik Çeviri

Otomatik Çeviri

本文提出了一种利用光致硫醇烯/硫醇-yne hydrothiolation 构建硫醚类/乙烯基硫化物栓系螺旋肽的协议。

Etiketler

ThioetherVinyl SulfideHelical PeptidesPhoto-induced Thiol-ene/yne Hydro-thiolationRink Amide MBHA ResinFmoc DeprotectionHCTUDIPEATrityl DeprotectionSolid-phase Peptide Synthesis

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