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挥发和氧化敏感的化合物使用冷进气系统和电子轰击质谱分析

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Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry

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挥发和氧化敏感的化合物使用冷进气系统和电子轰击质谱分析

9,504 Views

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05:48 min

•

September 05, 2014

DOI:

10.3791/51858-v

DOI:

10.3791/51858-v

•

05:48 min

September 05, 2014

•

4 Views

Jens Sproß¹

¹Department of Chemistry, Institute of Organic Chemistry,Bielefeld University

Özet

这部影片提出了一个协议，用电子轰击电离挥发和氧化敏感的化合物的质量spectrometrical分析。所提出的技术是为无机化学家兴趣尤其，与金属organyls，硅烷，或具有使用惰性条件下，例如在的Schlenk技术进行处理phosphanes工作。

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