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Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry
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JoVE Journal Chemistry
Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry

Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry

English

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9,504 Views

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05:48 min

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September 05, 2014

DOI:

10.3791/51858-v

DOI:
10.3791/51858-v

•

05:48 min
September 05, 2014

•

4 Views
1Department of Chemistry, Institute of Organic Chemistry,Bielefeld University

Summary

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This video presents a protocol for the mass spectrometrical analysis of volatile and oxidation sensitive compounds using electron impact ionization. The presented technique is especially of interest for inorganic chemists, working with metal organyls, silanes, or phosphanes which have to be handled using inert conditions, such as the Schlenk technique.

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Volatile CompoundsOxidation Sensitive CompoundsCold Inlet SystemElectron Impact Mass SpectrometrySector Field Mass SpectrometerAir-free ConditionsVacuum ConditionsMetal OrganylsSilanesPhosphanesSchlenk TechniqueInorganic Chemistry

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Cite this Article

Sproß, J. Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry. J. Vis. Exp. (91), e51858, doi:10.3791/51858 (2014).

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