Fracture and fragmentation are late stage phenomena in dynamic loading scenarios and are typically studied using explosives. We present a technique for driving expansion using a gas gun which uniquely enables control of both loading rate and sample temperature.
The dynamic fracture of a body is a late-stage phenomenon typically studied under simplified conditions, in which a sample is deformed under uniform stress and strain rate. This can be produced by evenly loading the inner surface of a cylinder. Due to the axial symmetry, as the cylinder expands the wall is placed into a tensile hoop stress that is uniform around the circumference. While there are various techniques to generate this expansion such as explosives, electromagnetic drive, and existing gas gun techniques they are all limited in the fact that the sample cylinder must be at room temperature. We present a new method using a gas gun that facilitates experiments on cylinders from 150 K to 800 K with a consistent, repeatable loading. These highly diagnosed experiments are used to examine the effect of temperature on the fracture mechanisms responsible for failure, and their resulting influence on fragmentation statistics. The experimental geometry employs a steel ogive located inside the target cylinder, with the tip located about halfway in. A single stage light gas gun is then used to launch a polycarbonate projectile into the cylinder at 1,000 m/sec-1. The projectile impacts and flows around the rigid ogive, driving the sample cylinder from the inside. The use of a non-deforming ogive insert allows us to install temperature control hardware inside the rear of the cylinder. Liquid nitrogen (LN2) is used for cooling and a resistive high current load for heating. Multiple channels of upshifted photon Doppler velocimetry (PDV) track the expansion velocity along the cylinder enabling direct comparison to computer simulations, while High speed imaging is used to measure the strain to failure. The recovered cylinder fragments are also subject to optical and electron microscopy to ascertain the failure mechanism.
The dynamic failure of a material is an important aspect of its overall mechanical behavior, and has relevance to numerous industries including automotive, aerospace, and military to name a few. While failure at low strain-rates is typically studied through conventional tension tests, in which a long thin sample is loaded in tension from the ends, at high strain rates such a geometry/configuration requires a sample to be very small in order to maintain a pseudo-mechanical equilibrium throughout the test. At the appearance of a single crack, the surrounding material will be relaxed, effectively arresting the development of any adjacent failure sites. This limits the number of fractures that can be simultaneously observed in any one experiment, and prevents important information regarding the statistics of failure to be determined.
The expanding cylinder test is a well-established technique for characterizing the manner in which materials fail and fragment under high speed loading. In the test, a cylinder made of the material of interest is uniformly loaded along its inner circumference, launching a stress wave through the wall and causing the cylinder to expand. Soon this radial wave dissipates and a uniform tensile hoop stress around the circumference dominates. As the stress and strain rate is the same around the cylinder the fracture and fragmentation behavior is governed solely by the material’s properties. The test alleviates the aforementioned problem as the typically large sample circumferences promote initiation of multiple failure sites under uniform stress 1.
The main aim in developing this experimental technique was to enable the study of the role of temperature in the fracture and fragmentation behavior of an expanding cylinder. The control of the sample temperature will allow for investigation of how the dynamic tensile strength, fracture mechanism, and fragmentation behavior of the material is affected. For example in metals, an increase in temperature can cause a shift from brittle to ductile fracture, accommodating more plastic work before ultimately failing. Some materials such as Ti-6Al-4V can also exhibit adiabatic shear localization 2. While the sample deforms, the plastic work generates heat. If the rate of softening as a result of this temperature increase is greater than the rate of work hardening from the deformation, an instability can form where a large amount of plastic deformation occurs in a very localized band (adiabatic shear band). This response is promoted in Ti-6Al-4V due to its poor thermal conductivity, and can potentially limit its effectiveness for applications such as lightweight armor.
This new testing approach must satisfy two main criteria. Firstly, the method must produce a radial strain rate on the order of 104 sec-1, typically seen in ballistic and impact events, to allow comparison to previous studies employing more traditional loading schemes. Secondly, the drive mechanism needs to be unaffected by the sample temperature to ensure consistency between experiments. Initial cylinder expansion mechanisms used explosive charges, either simply filling the sample cylinder 3-5 directly or using an intermediate driver. In the latter case a buffer is used 6, where the sample is placed over a steel cylinder that in turn contains an explosive charge. The obvious limitation is that as the sample cylinder contains the drive material (in the form of the explosive) heating the cylinder will also heat the charge. While this may not directly cause initiation of the charge many types of explosive contain a polymeric binder material that will melt out from the sample cylinder. Likewise, some explosives become highly sensitive when cooled. This means that explosive drives are not suitable for temperature study. An alternative method uses the Lorentz force for expansion — the sample is placed over a driver coil 7, 8. A high current is injected into this driver coil (typically heavy gauge copper wire), inducing an opposite current in the sample. These opposing currents have associated magnetic fields which act against each other, the magnetic pressure driving the sample outwards from the inner face. Again, heating the material will adversely affect the copper drive coil inside the sample. Gas guns have been used for cylinder expansion since the late 1970s 9. In these experiments the material used for the insert in the cylinder is a polymer, the drive coming as a result of both the projectile and insert deforming at impact. This insert is typically a rubber or plastic 10, the strength and ductility of which will be severely affected by temperature. Heating will make the insert too soft, and cooling will make it behave in a brittle manner so it fails prematurely.
Unlike previous cylinder expansion techniques, the method described here is the first to provide a repeatable loading drive over a wide range of temperatures (100-1,000 K). Our technique is unique in the fact that the material used for driving the expansion (in our case the projectile) is separate from the cylinder until the point of impact. Consequently, it is unaffected by the initial temperature of the sample cylinder and provides a repeatable load.
The experimental geometry consists of a steel ogive mounted inside the target cylinder, with the tip located about halfway along the length of the cylinder. A single stage light gas gun is then used to launch a polycarbonate projectile with a concave face into the cylinder at velocities up to 1,000 m/sec-1. The axis of the target is cylinder is carefully aligned to the axis of the gas-gun barrel to facilitate a repeatable and uniform load. The impact and subsequent flow of the polycarbonate projectile around the pseudo-rigid steel ogive, drives the cylinder into expansion from the inside wall. The geometry of the ogive insert and the concave face of the projectile were carefully optimized using hydro-code computer simulations to generate the desired expansion of the cylinder. Using 4340 alloy steel for the ogive enables experimentation with the cylinder at temperature as its strength is much higher than the polycarbonate projectile over the temperature range of interest, ensuring the drive mechanism remains consistent. Ogives recovered from heated and cooled experiments only exhibit minimal deformation as a result of the impact.
The heating and cooling of the sample cylinder is accomplished by the installation of temperature control hardware into a machined recess in the rear of the ogive insert. For cooling the sample to cryogenic temperatures (~100 K), the recess in the ogive is sealed with an aluminum cap and liquid nitrogen is flowed through the cavity. As the target cylinder has a large contact area with the ogive the sample is cooled through conduction. To heat the target cylinder to temperatures approaching 1,000 K, a ceramic and NiChrome resistive heater is placed in the ogive recess. A high current power supply provides up to 1 kW, heating the ogive and cylinder. The cylinder and ogive are thermally isolated from the target mount in the single stage gas-gun through the use of MACOR ceramic spacers. The tank is also held under moderate vacuum (<0.5 Torr) during the experiment which aids thermal manipulation.
In order to diagnose the fragmentation process of the cylinder, the experimental design includes multiple channels of frequency-conversion PDV, to measure the expansion velocity at points along the cylinder. PDV is a relatively new 11, optical fiber based interferometry technique which enables the measurement of surface velocities during highly dynamic events. During a PDV measurement, Doppler shifted light reflected from a moving surface of interest using a fiber-optic probe is combined with un-shifted light, creating a beat frequency that is directly proportional to the velocity of the moving surface. Essentially, a PDV system is a fast Michelson interferometer using advances in near-infrared (1,550 nm) communications technology to record beat frequencies in the GHz range. The mounting system for the 100 mm focal length PDV probes used in the current study ensures that they are isolated from the temperature of the cylinder and provides easy alignment. An additional advantage of using the 100 mm focal length probes is that they provide sufficient optical access to enable high speed photography to measure the expansion profile of the whole cylinder. The arrangement and location of the four probes, A-D, along the cylinder is shown in Figure 1. Two high speed cameras are employed here; a high speed video camera Phantom V16.10 operating at 250,000 fps and an IVV UHSi 12/24 framing camera, capturing 24 images. The IVV camera is backlit such that the cylinder is illuminated in silhouette enabling the radially expanding edge of the cylinder to be accurately tracked. The Phantom camera is front illuminated imaging the failure initiation and fragmentation process. The high speed photography can then be correlated with the velocimetry to give strain and strain rate along the full sample. The high speed imaging also allows for an accurate measure of failure strain and the fracture patterns along the surface.
The experimental technique presented in the following protocol section provides a means of controlling the sample temperature in an expanding cylinder experiment, through which different fracture mechanisms may be activated or suppressed. This technique will lead to a more comprehensive understanding of the role of temperature in dynamic loading scenarios.
1. Target Fabrication and Assembly
2. Gas Gun Preparation
3. Firing Preparation
4. Post Shot
5. Data Analysis
The quality of the data will firstly depend on the experimental timing. If the delays from trigger to impact are correct then the flash lamps will be producing enough light when the target cylinder begins to deform, enabling the high speed cameras to produce clear images. In this case the images from the framing camera will have a clear silhouetted edge that can be used to track the deformation of the whole cylinder. Software such as ImageJ can be used to extract lineout data for each frame, producing an image as in Figure 2. Ideally the PDV will be able to track the expansion velocity for ~100 µsec, this will depend on the surface finish of the cylinder and the alignment of the probe. For a given experiment the PDV and lineout data can be validated against one another using the four known points from the PDV in the image. With this combination an accurate measure of the radius or radial strain at any point along the cylinder length can be extracted. Figure 3 plots the radial expansion velocity at two points along the length of the cylinder, comparing experiments at 150 K and 800 K. We can see that the cooled cylinder has less deceleration after the peak velocity, suggesting fracture has initiated earlier leading to a loss of strength in the cylinder. The radial velocity is then integrated over time to reduce the radial displacement at the points observed by the probes. Figure 4 shows an example of this for the cooled cylinder. Images from the high speed video should be clear enough to discern fracture initiation and crack propagation, as seen in Figure 5. From this we extract the temporal activation of fracture and must extrapolate the number of cracks around the cylinder with time as the other side of the cylinder is not visible to the camera. Figure 5 is an example of a well-lit image, showing multiple longitudinal fractures along the cylinder.
The attached videos are examples of how the image quality is affected by the frame rate — a smaller interframe time produces more accurate time of fracture but the reduced resolution can make it difficult to accurately track crack propagation. The amount of compromise in this area will be determined by the camera hardware available, the lighting and lenses and the rate of deformation in the cylinder (i.e. the timescale that the fragmentation process occurs over).
Figure 1: Experimental geometry. Top, left: Basic assembly, showing location of PDV probes along the cylinder. Top, right: Ogive modifications for cooling and heating the cylinder. Bottom: Heated cylinder experiment installed on the gas gun. Black cables are power for the heating coil. Thin black/white cables are thermocouples. PDV probes are visible at the bottom. Please click here to view a larger version of this figure.
Figure 2: Lineout data extracted from high speed imaging of a 300 K expanding cylinder experiment at a range of times after impact.
Figure 3: Radial expansion velocity measured with PDV at two points along the cylinder for a 150 K (solid) and 800 K (dotted) expanding cylinder. The cooled cylinder has less deceleration after the peak velocity suggesting fracture has initiated earlier.
Figure 4: 150 K expanding cylinder. Solid lines: radial strain accumulated at 4 points along the cylinder length. Dotted lines: number of visible fracture sites from the high speed camera data.
Figure 5: Extract from high speed video (Video 1) recorded. 150 K expanding cylinder.
Video 1: High speed video of an expanding 150 K cylinder experiment. Projectile velocity 1,000 m/sec. Framing: 1 image every 10 µsec, 0.7 µsec exposure. Please click here to view this video.
Video 2: High speed video of an expanding 650 K cylinder experiment. Projectile velocity 1,000 m/sec. Framing: 1 frame every 4.7 µsec, 0.7 µsec exposure. Please click here to view this video.
This method enables investigation of materials at high rates of tensile loading over a wide range of temperatures, from cryogenic to ~1,000 K, unique to this design. However, this adds certain challenges to the experimental setup and execution. Firstly, to optimize the temperature control the ogive insert needs to be machined from a suitable material. 4340 steel is used here, although any high-temperature high-hardness steel should suffice. Likewise, as the entire expansion drive is now originating from the polymer projectile this needs to be made from a non-brittle plastic such as the machine-grade polycarbonate in this work.
It is important to have a close mechanical fit between the insert and the cylinder, to ensure good thermal contact. Care must be taken if the thermal expansion coefficient of the target cylinder is not close to the insert. For example, if the cylinder is brittle with a low thermal expansion (such as a ceramic) the expansion of the insert could damage or even crack the cylinder. For the same reason the epoxy used to bond the thermocouples on the cylinder must be able to resist the temperatures expected and the movement of the cylinder as it heats/cools. Finally, thermal isolation of the target from the mounting system is important, otherwise thermal soak makes temperature control difficult and can begin to adversely affect the PDV probes and target alignment.
The limitations of this technique are dependent on the projectile launching facilities available. The radial strain rates that can be attained are a function of the projectile velocity and the cylinder diameter. Smaller cylinders need lower projectile velocities but can then limit the number of fractures observed. Accurate measurement of the expansion velocity necessitates a quality laser based velocimetry system such as the upshifted PDV here or a multiple point VISAR.
Future applications are the study of the effects of temperature on the fracture mechanisms and resulting fragmentation behavior of materials at high rates of uniform tensile strain. While the experiment is especially suited to metals due to the reflective surface allowing PDV measurements it could be adapted to a range of materials if the surface is prepared correctly. This work at high and low temperatures is currently unavailable for other drive mechanisms for expanding cylinders, and will compliment other tensile test mechanisms allowing for further and more accurate population/calibration of material models and hydrocodes.
The authors have nothing to disclose.
The authors gratefully acknowledge continued funding and support for the project from the Atomic Weapons Establishment, AWE Plc. (UK) and Imperial College London.
Item | Company / Manufacturer | Part Number | Comments / Description |
1550 nm CW Laser | NKT Photonics | Koheras Adjustik | x 2 |
1550 nm Power Amplifier | NKT Photonics | Koheras Boostik HPA | |
Delay Generators | Quantum Composers | 9500+ Digital Delay Pulse Generator | 8 output version |
Stanford Research Systems | DG535 Digital Delay Generator | ||
16 Channel Digitiser | Agilent Technologies | U1056B Chassis + 4 X U1063A Digitiser | |
High Bandwidth Oscilloscopes | Teledyne LeCroy | WaveMaster 816Zi-A | Expansion Velocity, Gen 3 PDV |
Tektronix | DPO71604C | Projectile Velocity, Gen 1 PDV | |
High Speed Imaging Systems | Vision Research | Phantom v16.10 | |
Invisible Vision | IVV UHSi-24 | ||
Zeiss Optics | Planar T* 1,4/85 | 85mm Prime Lens | |
Nikon | AF-S Nikkor 70-200mm f/2.8 ED VR II | 70-200mm Telephoto Lens | |
Flash Lamp | Bowens | Gemini Pro 1500W | x 2 |
PDV Probe | Laser 2000 | LPF-04-1550-9/125-S-21.5-100-4.5AS-60-3A-3-3 | x 4 (Custom order) |
PDV System | Built in-house by the Institute of Shock Physics | Custom Build | 3rd Generation (Upshifted) 8 Channel Portable PDV System |
Control Software | National Instruments | LabVIEW 2013 | |
Control Hardware for heating | National Instruments | NI-DAQ 6009 USB | |
Heating Power Supply | BK Precision | BK1900 | |
Thermocouple Logger | Pico Technology | TC-08 | |
100 mm Single Stage Light Gas Gun | Physics Applications, Inc. (PAI) | Custom Build | Capable of at least 1000 meters per second with ~ 2 kg projectile |
Image analysis software | National Institutes of Health | ImageJ | Open source, free |
Image analysis software | Mathworks | MATLAB r2014a | With image processing toolboxes |
Material sectioning saw | Struers | Accutom-50 | |
Electron Microscope | Zeiss | Auriga | |
Electron Backscatter Diffraction | Bruker | e-Flash 1000 | |
EBSD software | Bruker | eSprit |