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通过超硫酸盐促进的β、β-不饱和化合物和烷基奈的苯基的高效合成在水中的多功能苯

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Química

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JoVE Journal Química

Efficient Synthesis of Polyfunctionalized Benzenes in Water via Persulfate-promoted Benzannulation of α,β-Unsaturated Compounds and Alkynes

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通过超硫酸盐促进的β、β-不饱和化合物和烷基奈的苯基的高效合成在水中的多功能苯

DOI:

10.3791/60767-v

•

05:34 min

•

December 16, 2019

•

Gabriela F. P. de Souza, Airton G. Salles

¹Department of Organic Chemistry, Institute of Chemistry,University of Campinas

Capítulos

00:04Título
00:37Benzannulation Reaction Employing Alkynes and α,β-unsaturated Compounds
02:02Extraction Workup and Purification
03:57Results: ¹H and ¹³C NMR
04:31Conclusion

Summary

Tadução automática

报道了水中对β、β-不饱和化合物和烷基化合物的超硫酸盐促进的无金属苯化，以合成前所未有的多功能化苯。

Tags

Keywords: Polyfunctionalized Benzenes Persulfate-promoted Benzannulation α β-unsaturated Compounds Alkynes Water As Solvent Sustainable Organic Chemistry Phenol Acetylene 2-cyclohexene-1-one Ammonium Persulfate Column Chromatography TLC Analysis

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