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利用过渡金属催化的酮的微波辅助直接异化
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A Microwave-Assisted Direct Heteroarylation of Ketones Using Transition Metal Catalysis
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利用过渡金属催化的酮的微波辅助直接异化

DOI:
10.3791/60441-v

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07:06 min

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February 16, 2020

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, , , , , , , , ,
1Department of Chemistry & Biochemistry,Northern Kentucky University

Capítulos

  • 00:05Introduction
  • 00:52Preparation of Reagents and Supplies for Glove Box Usage
  • 02:16Microwave Irradiation
  • 03:03Product Isolation
  • 05:32Results: 1H and 13C NMR Spectra and Flash Chromatography Purification Plot
  • 06:33Conclusion

Summary

Tadução automática

Tadução automática

杂性化合物是有机合成、药用和生物化学中的重要分子。微波辅助异质化，使用铂催化提供了一种快速而有效的方法，将异丙烯基直接附着在酮基材上。

Tags

Microwave-assistedHeteroarylationKetonesTransition Metal CatalysisPalladium CatalystAromatase InhibitorHormone Receptor-positive Breast CancerTert-butoxideTolueneXPhos Palladacycle CatalystAcetophenone3-iodopyridineMicrowave ReactorInfrared SensorReaction TemperatureSeparatory FunnelEthyl AcetateAmmonium Chloride

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