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35-吡啶N-氧化物脱水的合成、结晶和光谱表征
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JoVE Journal Química
Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate
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35-吡啶N-氧化物脱水的合成、结晶和光谱表征

8,211 Views

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06:18 min

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April 24, 2018

DOI:

10.3791/57233-v

DOI:
10.3791/57233-v

•

06:18 min
April 24, 2018

•

1 Views
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1Centro de Química, Instituto de Ciencias,Benemérita Universidad Autónoma de Puebla

Summary

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在此, 我们报告的合成和结晶的 35-吡啶n-氧化物脱水的一个简单的协议, 不同于经典合成吡啶N氧化物。该协议采用不同的起始材料, 反应时间较少, 产生一种新的溶解超分子结构, 在缓慢蒸发下结晶。

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Merino-García, R., Hernández-Anzaldo, S., Reyes-Ortega, Y. Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate. J. Vis. Exp. (134), e57233, doi:10.3791/57233 (2018).

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