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Capitoli
- 00:04Titolo
- 01:14Reaction
- 02:19Basicity Adjustment and Extraction
- 03:17Crystallization Process and Analysis of 3,5-Lutidine N-oxide Dehydrate
- 04:25Results: Characterization of 3,5-Lutidine N-Oxide Dehydrate
- 05:51Conclusion
Herein, we report the synthesis and crystallization of 3,5-lutidine N-oxide dehydrate by a simple protocol that differs from the classical synthesis of pyridine N-oxide. This protocol utilizes different starting material and involves less reaction time to yield a new solvated supramolecular structure, which crystallizes under slow evaporation.
Tags
Keywords: 35-lutidine N-oxide DehydrateSolvated Supramolecular StructureSynthetic Organic ChemistryInorganic Chemistry2-aminopyridine-35-dicarboxylic AcidGlacial Acetic Acid35-dimethylpyridineHydrogen PeroxideHigh-vacuum DistillationSodium CarbonateChloroformSodium SulfateDiethyl EtherCrystallization
