Journal
/
Química
/
Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations
JoVE Journal
Química
É necessária uma assinatura da JoVE para visualizar este conteúdo.  Faça login ou comece sua avaliação gratuita.
JoVE Journal Química
Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations

Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations

DOI:
10.3791/56897-v

•

13:09 min

•

January 04, 2018

•

, ,
1Department of Chemistry,National University of Singapore

Capítulos

  • 00:05Título
  • 00:53Sonogashira Coupling with Acetylene Gas
  • 05:17Photo-mediated Alkylation
  • 07:41Photo-redox Catalysis Fed by Acetylene Gas
  • 10:26Results: Reaction Optimization Using SFMT Reactors
  • 12:07Conclusion

Summary

Tadução automática

Tadução automática

A protocol for organic reaction screening using stop-flow micro-tubing (SFMT) reactors employing gaseous reactants and/or visible-light mediated reactions is presented.

Tags

Stop-flow Micro-tubing ReactorContinuous Flow ReactorBatch ReactorOrganic TransformationsReaction ScreeningGreen ChemistryPFA TubingBack Pressure Regulator4-iodoanisolePalladium CatalystDIPEADMSOSyringe PumpAcetylene Gas

Article

Embed

ADICIONAR À PLAYLIST

Usage Statistics

Vídeos Relacionados

Preparation of Hydrophobic Metal-Organic Frameworks via Plasma Enhanced Chemical Vapor Deposition of Perfluoroalkanes for the Removal of Ammonia

Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry

Chemical Vapor Deposition of an Organic Magnet, Vanadium Tetracyanoethylene

Synthesis of Cyclic Polymers and Characterization of Their Diffusive Motion in the Melt State at the Single Molecule Level

Synthesis of a Water-soluble Metal–Organic Complex Array

Using Capillary Electrophoresis to Quantify Organic Acids from Plant Tissue: A Test Case Examining Coffea arabica Seeds

Controlled Photoredox Ring-Opening Polymerization of O-Carboxyanhydrides Mediated by Ni/Zn Complexes

Surface Functionalization of Metal-Organic Frameworks for Improved Moisture Resistance

Development of Heterogeneous Enantioselective Catalysts using Chiral Metal-Organic Frameworks (MOFs)

Efficient Synthesis of Polyfunctionalized Benzenes in Water via Persulfate-promoted Benzannulation of α,β-Unsaturated Compounds and Alkynes

Read Article