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Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations
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Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations

Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations

DOI:
10.3791/56897-v

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13:09 min

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January 04, 2018

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, ,
1Department of Chemistry,National University of Singapore

Capitoli

  • 00:05Titolo
  • 00:53Sonogashira Coupling with Acetylene Gas
  • 05:17Photo-mediated Alkylation
  • 07:41Photo-redox Catalysis Fed by Acetylene Gas
  • 10:26Results: Reaction Optimization Using SFMT Reactors
  • 12:07Conclusion

Summary

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A protocol for organic reaction screening using stop-flow micro-tubing (SFMT) reactors employing gaseous reactants and/or visible-light mediated reactions is presented.

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Keywords: Stop-flow Micro-tubing ReactorContinuous Flow ReactorBatch ReactorOrganic TransformationsReaction ScreeningGreen ChemistryPFA TubingBack Pressure Regulator4-iodoanisolePalladium CatalystDIPEADMSOSyringe PumpAcetylene Gas

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