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Obtaining 3D Chemical Maps by Energy Filtered Transmission Electron Microscopy Tomography
JoVE Journal
Química
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JoVE Journal Química
Obtaining 3D Chemical Maps by Energy Filtered Transmission Electron Microscopy Tomography
DOI:

08:15 min

June 09, 2018

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Capítulos

  • 00:04Título
  • 01:35Alignment and Reconstruction of the Tilt Series
  • 03:38Quantification of Drift
  • 04:593D Chemical Mapping
  • 06:08Results: Reconstructed Models of Titania/Alumina Samples Provide Insight into Catalytic Applications
  • 07:05Conclusion

Summary

Tadução automática

This paper describes a protocol to achieve 3D chemical maps combining energy filtered imaging and electron tomography. The chemical distribution of two catalyst supports formed by elements that are difficult to distinguish by other imaging techniques was studied. Each application consists of mapping overlapped chemical elements - respectively spaced-ionization edges.

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