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Determining the Chemical Composition of Corrosion Inhibitor/Metal Interfaces with XPS: Minimizing Post Immersion Oxidation
Journal JoVE
Chimie
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Journal JoVE Chimie
Determining the Chemical Composition of Corrosion Inhibitor/Metal Interfaces with XPS: Minimizing Post Immersion Oxidation

Determining the Chemical Composition of Corrosion Inhibitor/Metal Interfaces with XPS: Minimizing Post Immersion Oxidation

DOI:
10.3791/55163-v

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07:44 min

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March 15, 2017

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, , , , ,
1Corrosion and Protection Centre, School of Materials,The University of Manchester, 2Laboratorio de Caracterización de Materiales Sintéticos y Naturales,Instituto Mexicano del Petróleo, 3Departamento de Metalurgia y Materiales,Instituto Politécnico Nacional

Chapitres

  • 00:05Titre
  • 01:16Preparation of Substrate in Inhibited Acid Solution
  • 01:57Sample Transfer to XPS Analysis Chamber
  • 04:03Acquisition of XPS Data
  • 05:12Results: Representative XPS Data from Carbon-steel Samples
  • 06:51Conclusion

Summary

Traduction automatique

Traduction automatique

A protocol to avoid the oxidation of metallic substrates during sample transfer from an inhibited acidic solution to an X-ray photoelectron spectrometer is presented.

Tags

Keywords: XPSCorrosion InhibitorMetal InterfacesOxidationSample TransferCarbon-steel SubstrateHydrochloric Acid SolutionInert GasGlove BoxRelative HumidityNitrile GlovesSample Preparation

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