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06:52 min
October 30, 2018
DOI:
10.3791/58803-v
采用改良的 Steglich 酯化反应, 合成了一个小的酯类衍生物与初级和二醇。该方法使用非卤化和更环保的溶剂, 乙腈, 并使产品在高产量的隔离, 而无需色谱纯化。
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Lutjen, A. B., Quirk, M. A., Kolonko, E. M. Synthesis of Esters Via a Greener Steglich Esterification in Acetonitrile. J. Vis. Exp. (140), e58803, doi:10.3791/58803 (2018).
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