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Achieving Moderate Pressures in Sealed Vessels Using Dry Ice As a Solid CO2 Source
Capítulos
- 00:04Título
- 00:50Reaction in a 7.5-mL Vial (Air Not Excluded)
- 02:33Reaction in a 7.5-mL Vial (Purging Conditions – Air Excluded)
- 03:34Reaction in a 35-mL Pressure Tube (Air Not Excluded)
- 05:08Results: Representative 1H NMR Reaction Analyses
- 05:46Conclusion
Here we present a protocol for performing reactions in simple reaction vessels under low-to-moderate pressures of CO2. The reactions can be performed in a variety of vessels simply by administering the carbon dioxide in the form of dry ice, without the need for costly or elaborate equipment or set-ups.
