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高效液相色谱-ESI-Q-MS 与红霉素通过光致降解法鉴定水生环境中的药物
JoVE Journal
Umwelt
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JoVE Journal Umwelt
Identification of Pharmaceuticals in The Aquatic Environment Using HPLC-ESI-Q-TOF-MS and Elimination of Erythromycin Through Photo-Induced Degradation
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高效液相色谱-ESI-Q-MS 与红霉素通过光致降解法鉴定水生环境中的药物

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05:46 min

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August 01, 2018

DOI:

10.3791/57434-v

DOI:
10.3791/57434-v

•

05:46 min
August 01, 2018

•

3 Views
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1Niederrhein University of Applied Sciences, 2University Duisburg-Essen

Summary

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我们提出了一个非目标分析的协议, 利用时间的飞行质谱作为一个完美的工具, 以识别水中的药物。我们演示了紫外线照射的应用, 以消除它们。对降解剖面的辐照、复合隔离、识别和动力学建模进行了分析。

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HPLC-ESI-Q-TOF-MSPharmaceuticalsAquatic EnvironmentErythromycinPhoto-induced DegradationSolid Phase ExtractionFiltrationRotary EvaporationNon-targeted AnalysisUV IrradiationPhotoreactorPH AdjustmentTime-course Sampling

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Voigt, M., Savelsberg, C., Jaeger, M. Identification of Pharmaceuticals in The Aquatic Environment Using HPLC-ESI-Q-TOF-MS and Elimination of Erythromycin Through Photo-Induced Degradation. J. Vis. Exp. (138), e57434, doi:10.3791/57434 (2018).

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