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Simple Methods for the Preparation of Non-noble Metal Bulk-electrodes for Electrocatalytic Applications
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化学
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JoVE 杂志 化学
Simple Methods for the Preparation of Non-noble Metal Bulk-electrodes for Electrocatalytic Applications

Simple Methods for the Preparation of Non-noble Metal Bulk-electrodes for Electrocatalytic Applications

DOI:
10.3791/56087-v

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09:18 min

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June 21, 2017

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, , , , , ,
1Faculty of Chemistry and Biochemistry, Inorganic Chemistry I,Ruhr-University Bochum, 2Fraunhofer Institute for Environmental, Safety, and Energy Technology, UMSICHT

Chapters

  • 00:05Title
  • 01:08High-temperature Synthesis of Fe4.5Ni4.5S8
  • 02:13Preparation of ‘Pellet’ Electrodes
  • 03:44Electrochemical Testing of Electrodes
  • 06:43Results: Preparation and Characterization of Rock and Pellet Electrodes Using Pentlandite
  • 08:26Conclusion

Summary

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A facile preparation method of electrodes using the bulk material Fe4.5Ni4.5S8 is presented. This method provides an alternative technique to conventional electrode fabrication and describes prerequisites for unconventional electrode materials including a straightforward electrocatalytic testing method.

Tags

Keywords: Non-noble Metal Bulk-electrodesElectrocatalytic ApplicationsElectrode Materials PreparationHydrogen Evolution ReactionBipedalitePentlandite Bulk MaterialSilver Epoxide GlueTeflon CasingBrass Rod

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