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Spark Plasma Sintering Apparatus Used for the Formation of Strontium Titanate Bicrystals
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工程学
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JoVE 杂志 工程学
Spark Plasma Sintering Apparatus Used for the Formation of Strontium Titanate Bicrystals

Spark Plasma Sintering Apparatus Used for the Formation of Strontium Titanate Bicrystals

DOI:
10.3791/55223-v

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11:17 min

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February 09, 2017

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,
1Department of Materials Science and Engineering,University of California, Davis

Chapters

  • 00:05Title
  • 00:50Strontium Titanate (SrTiO3) Single Crystal Sample Preparation
  • 01:54SrTiO3 Bicrystal Formation via a Spark Plasma Sintering (SPS) Apparatus
  • 03:44SrTiO3 Bicrystal Sample Preparation
  • 04:53TEM Sample Preparation via Focused Ion Beam (FIB) Milling
  • 09:08Results: Spark Plasma Sintering Apparatus-formed Strontium Titanate Bicrystals
  • 10:36Conclusion

Summary

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A viable technique for the formation of strontium titanate bicrystals at high pressure and fast heating rate via the spark plasma sintering apparatus is developed.

Tags

Spark Plasma SinteringStrontium Titanate BicrystalsGrain Boundary StructuresMisorientationCeramic ProcessingMicrostructure FormationSample PreparationDiamond Wire SawUltrasonic CleaningEtchingGraphite PaperGraphite DieUniaxial ForceThermocouple

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