A protocol is described for the characterization of the key electrochemical parameters of a boron doped diamond (BDD) electrode and subsequent application for in situ pH generation experiments.
Read, T. L., Macpherson, J. V. Assessment of Boron Doped Diamond Electrode Quality and Application to In Situ Modification of Local pH by Water Electrolysis. J. Vis. Exp. (107), e53484, doi:10.3791/53484 (2016).