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Quantitative Detection of Trace Explosive Vapors by Programmed Temperature Desorption Gas Chromatography-Electron Capture Detector
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Quantitative Detection of Trace Explosive Vapors by Programmed Temperature Desorption Gas Chromatography-Electron Capture Detector

Quantitative Detection of Trace Explosive Vapors by Programmed Temperature Desorption Gas Chromatography-Electron Capture Detector

19,479 Views

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07:57 min

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July 25, 2014

DOI:

10.3791/51938-v

DOI:
10.3791/51938-v

•

07:57 min
July 25, 2014

•

8 Views
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1Chemical Sensing & Fuel Technology, Chemistry Division,U.S. Naval Research Laboratory, 2NOVA Research, Inc., 3Bio/Analytical Chemistry, Chemistry Division,U.S. Naval Research Laboratory, 4Navy Technology Center for Safety and Survivability, Chemistry Division,U.S. Naval Research Laboratory

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Trace explosive vapors of TNT and RDX collected on sorbent-filled thermal desorption tubes were analyzed using a programmed temperature desorption system coupled to GC with an electron capture detector. The instrumental analysis is combined with direct liquid deposition method to reduce sample variability and account for instrumentation drift and losses.

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Quantitative DetectionTrace Explosive VaporsProgrammed Temperature DesorptionGas ChromatographyElectron Capture DetectorDirect Liquid DepositionSorbent-filled Thermal Desorption TubesVapor SamplesSolution StandardsVapor QuantitationNitro-energeticsTNTRDXElectron AffinityVapor Standards

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Field, C. R., Lubrano, A., Woytowitz, M., Giordano, B. C., Rose-Pehrsson, S. L. Quantitative Detection of Trace Explosive Vapors by Programmed Temperature Desorption Gas Chromatography-Electron Capture Detector. J. Vis. Exp. (89), e51938, doi:10.3791/51938 (2014).

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