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Die Synthese von [Sn<sub> 10</sub> (Si (SiMe<sub> 3</sub>)<sub> 3</sub>)<sub> 4</sub>]<sup> 2</sup<sup> -</sup> Eine metastabile Sn (I) halogenidlösung Verwendung über eine Co-Kondensationstechnik Synthetisierter
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The Synthesis of [Sn10(Si(SiMe3)3)4]2– Using a Metastable Sn(I) Halide Solution Synthesized via a Co-condensation Technique
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Die Synthese von [Sn<sub> 10</sub> (Si (SiMe<sub> 3</sub>)<sub> 3</sub>)<sub> 4</sub>]<sup> 2</sup<sup> -</sup> Eine metastabile Sn (I) halogenidlösung Verwendung über eine Co-Kondensationstechnik Synthetisierter

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12:43 min

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November 28, 2016

DOI:

10.3791/54498-v

DOI:
10.3791/54498-v

•

12:43 min
November 28, 2016

•

7 Views
, ,
1Chemistry Department, Institute of Inorganic Chemistry,University of Tübingen

Summary

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The disproportionation reaction of a metastable Sn(I) chloride solution, obtained via the preparative co-condensation technique, is used for the synthesis of a metalloid tin cluster compound.

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Binder, M., Schrenk, C., Schnepf, A. The Synthesis of [Sn10(Si(SiMe3)3)4]2- Using a Metastable Sn(I) Halide Solution Synthesized via a Co-condensation Technique. J. Vis. Exp. (117), e54498, doi:10.3791/54498 (2016).

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