This video method describes the synthesis of high surface area, monolithic 3D graphene-based materials derived from polymer precursors as well as single layer graphene oxide.
Campbell, P. G., Worsley, M. A., Hiszpanski, A. M., Baumann, T. F., Biener, J. Synthesis and Functionalization of 3D Nano-graphene Materials: Graphene Aerogels and Graphene Macro Assemblies. J. Vis. Exp. (105), e53235, doi:10.3791/53235 (2015).