Here, we present a protocol with a sol-gel process to synthesize gold intercalated in the walls of mesoporous materials (GMS), which is confirmed to possess a mesoporous matrix with gold intercalated in the walls imparting great stability and recyclability.
Ji, Y., Caskey, C., Richards, R. M. Synthesis and Catalytic Performance of Gold Intercalated in the Walls of Mesoporous Silica. J. Vis. Exp. (101), e52349, doi:10.3791/52349 (2015).