We describe a beamline setup meant to carry out rapid two-dimensional x-ray fluorescence and x-ray microdiffraction mapping of single crystal or powder samples using either Laue (polychromatic radiation) or powder (monochromatic radiation) diffraction. The resulting maps give information about strain, orientation, phase distribution, and plastic deformation.
Stan, C. V., Tamura, N. Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples. J. Vis. Exp. (136), e57874, doi:10.3791/57874 (2018).