Spin Saturation Transfer Difference NMR (SSTD NMR): A New Tool to Obtain Kinetic Parameters of Chemical Exchange Processes

Mar&#237;a Teresa Quir&oacute;s; Colin Macdonald; Jes&uacute;s Angulo; Mar&iacute;a Paz Mu&#241;oz

doi:10.3791/54499

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Spin Transferência Saturação Diferença NMR (SSTD RMN): Uma nova ferramenta obter Kinetic Parâmetros de processos químicos de câmbio

JoVE Journal
化学

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JoVE Journal 化学

Spin Saturation Transfer Difference NMR (SSTD NMR): A New Tool to Obtain Kinetic Parameters of Chemical Exchange Processes

Spin Transferência Saturação Diferença NMR (SSTD RMN): Uma nova ferramenta obter Kinetic Parâmetros de processos químicos de câmbio

17,345 Views

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11:44 min

•

November 12, 2016

DOI:

10.3791/54499-v

DOI:

10.3791/54499-v

•

11:44 min

November 12, 2016

•

4 Views

María Teresa Quirós¹, Colin Macdonald^1,2, Jesús Angulo², María Paz Muñoz¹

¹School of Chemistry,University of East Anglia, ²School of Pharmacy,University of East Anglia

概要

A detailed protocol describing the SSTD NMR method is presented here to help new users apply this new method to obtain the kinetic parameters of their own systems undergoing chemical exchange.

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Spin Saturation Transfer Difference NMR (SSTD NMR)Chemical Exchange Kinetic Parameters Molecule Dynamics Organic Molecules Organometallic Molecules Rotational Variance Conformational Equilibrium Nitrogen Inversion Lignin Exchange Tautomerization Temperature Control Proton NMR STDDIFF Pulse Sequence 90 Degree Hard Pulse

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Spin Transferência Saturação Diferença NMR (SSTD RMN): Uma nova ferramenta obter Kinetic Parâmetros de processos químicos de câmbio

概要

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