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Preparation of DMMTAV and DMDTAV Using DMAV for Environmental Applications: Synthesis, Purification, and Confirmation
Journal JoVE
Environnement
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Journal JoVE Environnement
Preparation of DMMTAV and DMDTAV Using DMAV for Environmental Applications: Synthesis, Purification, and Confirmation
DOI:

06:23 min

March 09, 2018

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Chapitres

  • 00:04Titre
  • 00:48Dimethylmonothioarsinic Acid (DMMTAV) Synthesis
  • 03:23Dimethyldithioarsinic Acid (DMDTAV) Synthesis
  • 05:06Results: Characterization of DMMTAV and DMDTAV
  • 05:59Conclusion

Summary

Traduction automatique

This article presents modified experimental protocols for dimethylmonothioarsinic acid (DMMTAV) and dimethyldithioarsinic acid (DMDTAV) synthesis, inducing dimethylarsinic acid (DMAV) thiolation through mixing of DMAV, Na2S, and H2SO4. The modified protocol provides an experimental guideline, thereby overcoming limitations of the synthesis steps that could have caused experimental failures in quantitative analysis.

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