The disproportionation reaction of a metastable Sn(I) chloride solution, obtained via the preparative co-condensation technique, is used for the synthesis of a metalloid tin cluster compound.
Binder, M., Schrenk, C., Schnepf, A. The Synthesis of [Sn10(Si(SiMe3)3)4]2- Using a Metastable Sn(I) Halide Solution Synthesized via a Co-condensation Technique. J. Vis. Exp. (117), e54498, doi:10.3791/54498 (2016).